Hostname: page-component-54dcc4c588-sq2k7 Total loading time: 0 Render date: 2025-10-09T08:40:51.719Z Has data issue: false hasContentIssue false
  • English
  • Français

Pressure/Temperature/Reaction Phase Diagrams for Several Nitramine Compounds

Published online by Cambridge University Press:  15 February 2011

T. P. Russell ,
P. J. Miller ,
G. J. Piermarini  and
S. Block
T. P. Russell
Affiliation:
Naval Surface Warfare Center Silver Spring, Maryland 20903–5000
P. J. Miller
Affiliation:
Naval Surface Warfare Center Silver Spring, Maryland 20903–5000
G. J. Piermarini
Affiliation:
Materials Science and Engineering Laboratory National Institute of Standards and Technology Gaithersburg, Maryland 20899
S. Block
Affiliation:
Materials Science and Engineering Laboratory National Institute of Standards and Technology Gaithersburg, Maryland 20899
Get access

Abstract

Pressure/temperature/reaction phase diagrams for several nitramine compounds, including hexanitrohexaazaisowurtzitane (HNIW), 1,3,5-trinitrohexahydro-l,3,5-triazine (RDX), ammonium dinitramide (ADN), and p-nitroaniline (PNA) are presented. A diamond anvil cell was used in conjunction with optical polarizing light microscopy (OPLM), Fourier transform infrared spectroscopy (FTIR), energy dispersive X-ray diffraction (EDXD), and micro FT-Raman spectroscopy to determine these diagrams. A description is given of the diamond anvil cell and the associated techniques employed.

Information

Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 296: Symposium Y – Structure and Properties of Energetic Materials , 1992 , 199
Copyright
Copyright © Materials Research Society 1993

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

Article purchase

Temporarily unavailable

References

1. Gupta, Y. M., Shock Compression of condensed Matter. edited by Schmidt, S. C., Dick, R. D., Forbes, J. W., and Tasker, D. G. (Proceedings of the American Physical Society Topical Conference, Williamsburg, VA, 1991) pp. 15 and all included references.Google Scholar
2. Russell, T. P., Miller, P. J., Piermarini, G. J., Block, S., J. Phys. Chem, 96, 5509 (1992).Google Scholar
3. Russell, T. P., Miller, P. J., Piermarini, G. J., Block, S., J. Phys. Chem., (in press).Google Scholar
4. Piermarini, G. J., Block, S., Miller, P. J., The Chemistry and Physics of Energetic Materials, ed. by Bulusu, S., (NATO Advanced Study Institute, 309, Altavilla Milicia, Sicily, September 3–15, 1989), pp. 369–412.Google Scholar
5. Barnett, J. D.; Block, S.; Piermarini, G. J., Rev. Sci. Instrum., 44, 1 (1973).Google Scholar
6. Piermarini, G. J., Block, S., Barnett, J. D., and Forman, R. S., J. Appl. Phys., 46, 2774 (1975).Google Scholar
7. Block, S.; Piermarini, G. J., Physics Today, 29, 44 (1976).Google Scholar
8. Miller, P. J., Piermarini, G. J., Block, S., Appl. Spectrosc., 38, 680 (1984).Google Scholar
9. Miller, P. J., Block, S., Piermarini, G. J., Combustion and Flame, 83, 174 (1991).Google Scholar
10. Piermarini, G. J., Block, S., Barnett, J. D., J. Appl. Phys., 44, 5377 (1973).Google Scholar
11. Mauer, F. A., Block, S., Piermarini, G. J., American Crystallographic Association, Program and Abstracts of Summer Meeting, Boston University, Boston, MA Aug 12–17, Paper G3 (1979).Google Scholar
12. Weir, C. E., Lippincott, E. R., Van Valkenburg, A., and Bunting, E. N., J. Research NBS, 63A, 55 (1959).Google Scholar
13. Jamieson, J. C., Lawson, A. W., Nachtrieb, N. D., Rev. Sci. Instrum., 30, 1010 (1959).CrossRefGoogle Scholar
14. Piermarini, G. J. and Weir, C. E., J. Research NBS, 66A, 325 (1962).Google Scholar
15. Bassett, W. A., Takahashi, A. T., and Stook, P. W., Rev. Sci. Instrum., 38, 37 (1967).Google Scholar
16. Mao, H. K., and Bell, P. M., in Carnegie Institution of Washington Year Book, 77, 904 (1978).Google Scholar
17. Hirsh, K. R. and Holzapfel, W. B., Rev. Sci. Instrum., 52, 52 (1974).Google Scholar
18. Merrill, L., and Bassett, W. A., Rev. Sci. Instrum., 45, 209 (1974).Google Scholar
19. Russell, T. P. and Piermarini, G. J., presented at the FT-Raman Vibrational Spectroscopy Workshop, Bethesda, MD, May 1992 (unpublished), T. P. Russell and G.J. Piermarini, (to be published).Google Scholar
20. Giessen, B. C. and Gordon, G. E., Science, 159, 973 (1968).Google Scholar
21. Albritton, L. M. and Margrave, J. L., High Temperatures-High Pressures 4, 13 (1972).Google Scholar
22. Buras, B., Staun Olsen, J., Gerward, L., Selmark, B., and Lindegaard Andersen, A., Acta Cryst., A31, 327 (1975).Google Scholar
23. Russell, T. P., Piermarini, G. J., and Block, S., presented at ONR Workshop on AND, Arlington, VA, Feb. 1992 (unpublished), T. P. Russell, and G. J. Piermarini, S. Block, (to be published).Google Scholar
24. Block, S. and Piermarini, G. J., SPIE, 878, 21 (1988).Google Scholar
25. Yee, R. Y., Nadler, M. P., Neilson, A. T., JANNAF Proceeding, CPIA publication, October 1990.Google Scholar
26. Kraeutle, K. J., JANNAF Proceedings, CPIA publication #498, October 1988.Google Scholar
27. Kraeutle, K. J., JANNAF Proceedings, CPIA publication, November 1990.Google Scholar
28. Bridgman, P. W., Proc. Amer. Acad. Arts Sci. 51, 581 (1916).CrossRefGoogle Scholar
29. Russell, T. P., Stem, A. W., Koppes, W., and Bedford, C. D., JANNAF Proceedings, CPIA Publication #593, October 1992.Google Scholar